A method for determining shell in palm kernel cake (PKC) is described.
This simple and rapid method requires little pretreatment compared wi
th the method currently used in PKC trade, in which the sample undergo
es defatting, acid and alkali digestion, and washing, before a chlorof
orm-alcohol solution is used to separate the shells. In the proposed m
ethod, only defatting the sample is required, The shells are separated
by the density difference between the shell and PKC in a potassium io
dide solution. Recoveries of at least 93% were obtained, and the corre
lation coefficient between the actual shell content and the determined
shell content was 0.999, with gradients of 0.97 and 0.98 for fine and
coarse shell, respectively.