A NEW TRICYCLIC RING-SYSTEM - THE 1,4,8,1 1-TETRA-AZATRICYCLO(9,3,1,1(4,8))-HEXADECANE OBTAINED BY THE REACTION OF TETRAMETHYLDIAMINOMETHANE WITH A 1,4,8,11-TETRA-AZACYCLOTETRADECANE (CYCLAM) AND THE X-RAY STRUCTURE OF THE PRODUCT
T. Bailly et al., A NEW TRICYCLIC RING-SYSTEM - THE 1,4,8,1 1-TETRA-AZATRICYCLO(9,3,1,1(4,8))-HEXADECANE OBTAINED BY THE REACTION OF TETRAMETHYLDIAMINOMETHANE WITH A 1,4,8,11-TETRA-AZACYCLOTETRADECANE (CYCLAM) AND THE X-RAY STRUCTURE OF THE PRODUCT, Comptes rendus de l'Academie des sciences. Serie II. Mecanique, physique, chimie, astronomie, 322(2), 1996, pp. 151-154
In the course of our research about intermediates in the Kabachnik-Fie
lds reaction, the synthesis of the the novel 1,4,8,11-Tetra-azatricycl
o hexadecane (3) under bar from the 1,4,8,11-Tetra-azacyclotetradecane
(Cyclam) is reported; NMR and X-ray data confirm the structure of (3)
under bar.