STRUCTURE OF OXY-2-FLUOROPROPYL)-N-TERT-BUTYLBENZENESULFONAMIDE

Authors
KIM MJ LEE YB KIM DW LIM SS LEE JH RYU BY SUH IH
Citation
Mj. Kim et al., STRUCTURE OF OXY-2-FLUOROPROPYL)-N-TERT-BUTYLBENZENESULFONAMIDE, Acta crystallographica. Section C, Crystal structure communications, 50, 1994, pp. 103-106
Citations number
17
Categorie Soggetti
Crystallography
Journal title
Acta crystallographica. Section C, Crystal structure communications → ACNP
ISSN journal
01082701
Volume
50
Year of publication
1994
Part
1
Pages
103 - 106
Database
ISI
SICI code
0108-2701(1994)50:<103:SOO>2.0.ZU;2-N
Abstract
The structure of the title compound, C15H22FNO4S N-tert-butylsulfamoyl )-alpha-(1-fluoroethyl)benzyl acetatel, has been determined from a sin gle-crystal X-ray diffraction study. The torsion angles C(7)-O(1)-C(10 )-O(2) [2.5 (3)-degrees] and C(1)-S-N-H(N) [-62.6 (2)-degrees], and an intramolecular hydrogen bond between the N atom and O(2) [2.979 (4) a ngstrom] stabilize the structure. The structure analysis confirms oppo site configurations at C(7) and C(8). The absence of close contacts le ss than 3.269 (4) angstrom [C(11) ... F] shows that the molecules are bound by van der Waals forces.