M. Oliveira et Jd. Bolton, EFFECT OF CERAMIC PARTICLES ON THE MECHANICAL-PROPERTIES OF M3 2 HIGH-SPEED STEEL/, International journal of powder metallurgy, 32(1), 1996, pp. 37-49
New wear resistant materials were developed by adding TiC (6, 16 and 4
2 mu m), TiN (7 and 12 mu m) and TiO2 (12 mu m) particles to AISI M3/2
high speed steel powder containing copper-phosphide and graphite in o
rder to obtain composite mixtures sinterable in the temperature range
1140-1170 degrees C. This work presents the effects of the ceramic par
ticles on hardness, bend strength and fracture toughness of the compos
ites, as compared to those of the base material. Since ceramic particl
es acted as crack initiators and reduced bend strength, additions of f
iner particle sizes resulted in a higher average of bend strength valu
es (1.35G.Pa) than in composites containing coarser additions (1.17GPa
). The average bend strength of the base material was 1.40GPa. No sign
ificant increase in hardness was obtained by adding the hard particles
to the base material. Hardening and tempering caused a slight hardnes
s increase and could therefore be beneficial to wear resistance. The c
omposites containing TiO2 however were very porous and the hardness of
the particles decreased significantly due to their interaction with t
he matrix, making these additions unsuitable. Fracture toughness was n
ot affected significantly by the presence of the ceramic particles but
, heat treatment caused a decrease in fracture toughness from an avera
ge value of 16.5MPa m(1/2) in the as sintered condition to 13MPa m(1/2
) after hardening and tempering.