H-1 AND C-13 NMR ASSIGNMENTS FOR A 27-NOROLEAN-13-EN-3-HYDROXY-28-OICACID GLYCOSIDE FROM ISERTIA-HAENKEANA

Authors
RUMBERO A VAZQUEZ P BRUIX M
Citation
A. Rumbero et al., H-1 AND C-13 NMR ASSIGNMENTS FOR A 27-NOROLEAN-13-EN-3-HYDROXY-28-OICACID GLYCOSIDE FROM ISERTIA-HAENKEANA, Magnetic resonance in chemistry, 34(2), 1996, pp. 151-155
Citations number
15
Categorie Soggetti
Spectroscopy,Chemistry
Journal title
Magnetic resonance in chemistry → ACNP
ISSN journal
07491581
Volume
34
Issue
2
Year of publication
1996
Pages
151 - 155
Database
ISI
SICI code
0749-1581(1996)34:2<151:HACNAF>2.0.ZU;2-6
Abstract
A nortriterpene glycoside, pyrocincholic acid 3 oxy-D-glucopyranoside- 28-O-beta-D-glucopyranoside, was isolated from the leaves of Isertia h aenkeana and its structure established by H-1 and C-13 NMR spectral st udies. The complete H-1 and C-13 NMR resonance assignments for this tr iterpene were confirmed by the conventional 1D NMR methods and 2D shif t-correlated NMR techniques: DQF COSY, TOCSY, ROESY and HMQC.