L. Boudoukha et al., MECHANICAL CHARACTERIZATION BY NANOINDENTATION OF ZIRCONIUM ION-IMPLANTED ALUMINA, Nuclear instruments & methods in physics research. Section B, Beam interactions with materials and atoms, 108(1-2), 1996, pp. 87-93
Polycrystalline alpha-Al2O3 was implanted at 170 keV with doses of 2x1
0(16), 1x10(17) or 2x10(17) ions/cm(2). The as-implanted samples were
then annealed at 1000, 1200 and 1400 degrees C. The mechanical propert
ies, such. as hardness (H) and Young's modulus (E), of these ion-impla
nted samples were characterized by a depth-sensing low-load indentatio
n technique. The results showed that, with a low dose ion implantation
followed by annealing at 1200 degrees C, a significant increase in ha
rdness and elastic modulus were found. For higher doses, where the imp
lantation leads to the amorphisation of the material, the mechanical p
roperties of the implanted alumina were inferior to those of unimplant
ed alumina.