L. Kavan et al., NANOCRYSTALLINE TIO2 (ANATASE) ELECTRODES - SURFACE-MORPHOLOGY, ADSORPTION, AND ELECTROCHEMICAL PROPERTIES, Journal of the Electrochemical Society, 143(2), 1996, pp. 394-400
Ten different nanotextured TiO2 films were prepared from six commercia
l and four laboratory synthesized precursors. Krypton adsorption isoth
erms on the films and parent powders indicate the effect of sintering
and agglomeration. Electrochemical characterization of the films was a
imed at double-layer charging and Li+ insertion. The relations between
the film's morphology adsorption properties, and electrochemical beha
vior in the accumulation regime are discussed.