A study was made to determine the effect of chloride ion during electr
odeposition of copper, using an open-channel cell, Electrolysis parame
ters, such as current density, copper concentration, temperature, and
circulation rate were varied in the presence of chloride ion to determ
ine their effect, The deposits were examined by scanning electron micr
oscopy (SEM) and X-ray diffractometry (XRD) to determine morphology an
d crystallographic orientations, It was observed that chloride ion aff
ects the quality of the deposit surface, crystallographic orientations
and deposit morphology of cathode copper, These are further affected
by changing the electrolysis parameters.