P. Jonas et P. Schattschneider, THE EXPERIMENTAL CONDITIONS FOR COMPTON-SCATTERING IN THE ELECTRON-MICROSCOPE, Journal of physics. Condensed matter, 5(39), 1993, pp. 7173-7188
Electron Compton scattering from solids (ECOSS) is a technique for obt
aining the momentum density distribution of charge carriers in a solid
on a scale of mum or less. We discuss the possibilities and the probl
ems of this experimental technique, which uses a conventional transmis
sion election microscope (CTEM) equipped with a parallel electron ener
gy-loss spectrometer (PEELS). Favourable experimental conditions are p
roposed, including a scattering geometry that minimizes contributions
from Bragg scattering. The procedures leading from raw spectra to Comp
ton profiles that can be compared with theoretical predictions are des
cribed, with emphasis on background handling and deconvolution. It is
shown that experiments agree well with theory. An ultimate momentum re
solution of 0.05 atomic units appears feasible.