Toxic metal ions (cadmium, nickel and zinc), considered as priority po
llutants, were removed from dilute aqueous solutions by sorption onto
non-living (sterilized) anaerobically digested sewage sludge. The deso
rption of cadmium from metal-laden sludge was also examined. Flotation
was subsequently applied as an effective solid/liquid separation proc
ess. The dissolved-air flotation technique was applied for the generat
ion of fine bubbles and, in parallel, electrokinetic measurements were
carried out. Promising results were succeeded from the combined proce
ss of biosorption/flotation (termed biosorptive flotation).