X. Huang et al., EFFECT OF HOMOGENIZATION HEAT-TREATMENT ON THE MICROSTRUCTURE AND HEAT-AFFECTED ZONE MICROFISSURING IN WELDED CAST ALLOY-718, Metallurgical and materials transactions. A, Physical metallurgy andmaterials science, 27(3), 1996, pp. 785-790
The effect of homogenization temperature on microfissuring in the heat
-affected zones of electron-beam welded cast INCONEL 718 has been stud
ied. The material was homogenized at various temperatures in the range
of 1037 degrees C to 1163 degrees C and air-cooled The homogenized ma
terial was then electron-beam welded by the bead-on-plate welding tech
nique. The microstructures and microfissuring in the heat-affected zon
e (HAZ) were evaluated by analytical scanning electron microscopy (SEM
). The grain boundary segregation of various elements was evaluated by
secondary ion mass spectroscopy (SIMS). It was observed that the tota
l crack length (TCL) of microfissures first decreases with homogenizat
ion temperature and then increases, with a minimum occurring in the sp
ecimen heat treated at 1163 degrees C. This trend coincides with the v
ariation in segregation of B at grain boundaries with homogenization t
emperature and has been explained by equilibrium and nonequilibrium se
gregation of B to grain boundaries during the homogenization heat trea
tment. No other element was observed to segregate at the grain boundar
ies. The variation in volume fraction of phases like delta-Ni3Nb, MC c
arbide, and Laves phases does not follow the same trend as that observ
ed for TCL and B segregation at the grain boundaries. Therefore, micro
fissuring in HAZ of welded cast INCONEL 718 is attributed to the segre
gation of B at the grain boundaries.