Application of compounds which, on textile material, release small qua
ntities of formaldehyde makes it necessary to develop an adequate anal
ytical method. Polarography is one of the possible analytical methods
to be used. This paper investigates the possibility of using an indire
ct DC polarographic method via semicarbazone, with direct extraction o
f formaldehyde in the polarographic cell. Such a modified polarographi
c method is highly sensitive and selective, it makes it possible to me
asure small quantities of formalhyde, while the maximum sample mass to
be measured is around 0.2 g. Disturbances that presumably occur due t
o the presence of surface active agents on the textile material do not
occur in the samples smaller than 0.2 g in 30 ml of the polarographic
solution.