V. Randle et al., THE DEFORMATION-BEHAVIOR OF GRAIN-BOUNDARY REGIONS POLYCRYSTALLINE ALUMINUM, Philosophical magazine. A. Physics of condensed matter. Structure, defects and mechanical properties, 73(2), 1996, pp. 265-282
The deformation pattern at grain boundaries and at triple junctions in
polycrystalline high purity aluminium (99.999%) has been studied by e
lectron back scattering pattern (EBSP) observations. Specimens of two
different grain sizes rolled to give 5% and 30% reductions have been e
xamined by these different EBSP scans: (i) scans across grain boundari
es, (ii) scans along grain boundaries and (iii) two-dimensional scans
near triple junctions. These scans are carried out in small steps (1-5
mu m) over long distances (up to 50 mu m). The EBSP measurements show
that the level of perturbations increases with strain and that enhanc
ed zones of perturbations are observed at grain boundaries and especia
lly near triple junctions. In specimens deformed by 30%, such zones of
large perturbation are observed at most of the grain boundaries, and
in the specimens deformed by 5%, at some triple junctions. The EBSP me
asurements are compared to previous microstructural observations by tr
ansmission electron microscopy and the effect of the zones of enhanced
perturbations is discussed with relation to the mechanical and therma
l behaviour at highly deformed polycrystalline metals.