CHROMATOGRAPHIC RESOLUTION OF SEVERAL RACEMIC 9-FLUORENYL DERIVATIVESON A BONDED CELLULOSE DERIVED CHIRAL STATIONARY-PHASE FOR HPLC

Authors
VELASCO D YU ZR FRANCO P MINGUILLON C
Citation
D. Velasco et al., CHROMATOGRAPHIC RESOLUTION OF SEVERAL RACEMIC 9-FLUORENYL DERIVATIVESON A BONDED CELLULOSE DERIVED CHIRAL STATIONARY-PHASE FOR HPLC, Tetrahedron : asymmetry, 7(3), 1996, pp. 633-636
Citations number
7
Categorie Soggetti
Chemistry Inorganic & Nuclear","Chemistry Inorganic & Nuclear","Chemistry Physical
Journal title
Tetrahedron : asymmetry → ACNP
ISSN journal
09574166
Volume
7
Issue
3
Year of publication
1996
Pages
633 - 636
Database
ISI
SICI code
0957-4166(1996)7:3<633:CROSR9>2.0.ZU;2-A
Abstract
The enantiomers of several 9-fluorenyl derivatives have been successfu lly resolved by HPLC on a chiral stationary phase (CSP) based on a mix ed 10-undecenoate/3,5-dimethylphenylcarbamate of cellulose bonded to a llylsilica gel. Previous attempts at resolution, such as NMR methods, GC and the use of a multiple interaction type chiral column for HPLC, were unsuccessful. (C) 1996 Elsevier Science Ltd