C. Mayr et al., ANALYSIS OF DISLOCATION-STRUCTURES AFTER DOUBLE SHEAR CREEP DEFORMATION OF CMSX6-SUPERALLOY SINGLE-CRYSTALS AT TEMPERATURES ABOVE 1000-DEGREES-C, Materials science & engineering. A, Structural materials: properties, microstructure and processing, 207(1), 1996, pp. 51-63
Dislocation structures which form during pure shear creep deformation
of the superalloy single crystal alloy CMSX6 at 1025 degrees C under a
shear stress of 85 MPa were analysed using transmission electron micr
oscopy. Two macroscopic crystallographic shear systems were studied: {
111}[110] and {100}[010]. At the minimum creep rate (observed at shear
values of 0.02) the system {111}[110] deforms by a factor of ten fast
er than the system {100} on the basis of an external resolved shear st
ress argument. Shear creep deformation was always associated with mult
iple slip and nucleation of dislocations was not difficult (absence of
incubation periods for creep). A detailed study of dislocation networ
ks around gamma'-particles underlined the importance of [110]{111} gli
de and climb processes in the gamma-channels in the formation of these
networks. Microstructural parameters and processes which must be cons
idered to fully account for the mechanism of creep in superalloy SX ar
e outlined. Channel work hardening always preceded the cutting of gamm
a'-particles which started at the minimum creep rate.