POLYFLUORINATED HYDRAZONES IN ORGANIC-SYNTHESIS .2. OXIDATION OF ,5,5-HEXAFLUORO-4-TRIFLUOROMETHYLPENTANE-2,3-DIONE BISHYDRAZONE - SYNTHESIS AND STRUCTURE OF 4-(1,1,1,3,3,3-HEXAFLUOROISOPROPYL)-1,2,3-TRIAZOLE
Gg. Bargamov et al., POLYFLUORINATED HYDRAZONES IN ORGANIC-SYNTHESIS .2. OXIDATION OF ,5,5-HEXAFLUORO-4-TRIFLUOROMETHYLPENTANE-2,3-DIONE BISHYDRAZONE - SYNTHESIS AND STRUCTURE OF 4-(1,1,1,3,3,3-HEXAFLUOROISOPROPYL)-1,2,3-TRIAZOLE, Russian chemical bulletin, 44(12), 1995, pp. 2361-2363
Oxidation of N,N'-unsubstituted ,5,5-hexafluoro-4-trifluoromethylpenta
ne-2,3-dione bishydrazone with sulfuryl chloride or bromine in CCl4 gi
ves l-4-(1,1,1,3,3,3-hexafluoroisopropyl)-1,2,3-triazo in high yield.
Its structure has been confirmed by X-ray structural analysis.