An. Danilewsky et al., LONG-TERM CRYSTAL-GROWTH UNDER MICROGRAVITY DURING THE EURECA-1 MISSION .2. THM GROWTH OF SULFUR-DOPED INP, Crystal research and technology, 31(2), 1996, pp. 139-149
Long-term crystal growth experiments were successfully performed under
microgravity conditions during the first flight of the unmanned EUREC
A-1 mission in the automatic mirror furnace (AMF). Two crystals of sul
phur-doped InP with [001] and [111] orientation respectively were grow
n from indium solution by the travelling heater method (THM). The abse
nce of time dependent buoyancy-driven convection is documented by the
lack of type I striations in the space-grown crystals. The sulphur con
centration is measured by spatially resolved photoluminescence. As exp
ected, the macrosegregation can be described by a pure diffusion-contr
olled model which is in good agreement with the findings from the firs
t German spacelab mission D1. Compared to the earth-grown reference sa
mples, both of the space-grown InP crystals show strong disturbances s
uch as inclusions and type II striations. The morphological instabilit
ies are similar to growth disturbances already known from the space-gr
own MD-ELI-01 from the D1 mission.