A systematic procedure has been developed for feed-line aerated potati
on column evaluation in laboratory and plant. Slurry in batch operatio
n is continuously recirculated from the column bottom through an exter
nal aerator and then incremental froth products are collected. In cont
inuous operation, a grade-recovery curve is generated by changing feed
and gas rate. The selectivity data from these two modes of column ope
ration are compared. The experimental procedures are described in this
paper with an example application to chalcocite-heazlewoodite separat
ion at INCO's Matte Separation plant. The significance of the experime
ntal procedure for column design and scale-up as well as general colum
n testwork is discussed.