QUANTITATIVE-DETERMINATION OF COMPLETELY ACETYLATED PENTAERYTHRITOL AND PENTAERYTHRITOL OLIGOMERS BY HIGH-PERFORMANCE LIQUID-CHROMATOGRAPHY

Authors
TAPSAK MA WANG GH AZIZIAN K WEBER WP
Citation
Ma. Tapsak et al., QUANTITATIVE-DETERMINATION OF COMPLETELY ACETYLATED PENTAERYTHRITOL AND PENTAERYTHRITOL OLIGOMERS BY HIGH-PERFORMANCE LIQUID-CHROMATOGRAPHY, Analytical chemistry, 68(10), 1996, pp. 1685-1687
Citations number
20
Categorie Soggetti
Chemistry Analytical
Journal title
Analytical chemistry → ACNP
ISSN journal
00032700
Volume
68
Issue
10
Year of publication
1996
Pages
1685 - 1687
Database
ISI
SICI code
0003-2700(1996)68:10<1685:QOCAPA>2.0.ZU;2-M
Abstract
Analysis of pentaerythritol (PE) and PE oligomer mixtures has been ach ieved. PE oligomer mixtures are completely and rapidly (15 min) acetyl ated using acetic anhydride and a catalytic amount of 4-(dimethylamino )pyridine. A Whatman Partsil-10 C-8 HPLC column resolves acetylated PE oligomers, which include acetylated penta-PE, with a mobile phase of acetonitrile/water (1:1 v/v).