S. Ono et al., PROCESSING OF HIGHLY ORIENTED LINBO3 FILMS FOR WAVE-GUIDES FROM AQUEOUS-SOLUTION, Journal of the American Ceramic Society, 79(5), 1996, pp. 1343-1350
Stoichiometric and homogeneous LiNbO3 films were prepared by using a L
i and Nb hydroxide aqueous coating solution from a double alkoxide, In
this method, a double alkoxide precursor solution was hydrolyzed comp
letely to form the gel, which was subjected to dissolution into water
to form the aqueous coating solution, Processing with the aqueous coat
ing solution was preferable in terms of much less carbonic residue in
coated films than with the alkoxide ethanol solution, The coated films
crystallized with high orientation by subsequent heat-treatment at te
mperatures as low as 350 degrees C, Ti-doped (5 mol%) LiNbO3 homogeneo
us films (Ti:LiNbO3) were also prepared.