OPERATIONAL CHARACTERISTICS OF THE EVAPORATIVE LIGHT-SCATTERING DETECTOR USED IN ANALYSIS OF ETHOXYLATED ALCOHOLS

Authors
MISZKIEWICZ W SZYMANOWSKI J
Citation
W. Miszkiewicz et J. Szymanowski, OPERATIONAL CHARACTERISTICS OF THE EVAPORATIVE LIGHT-SCATTERING DETECTOR USED IN ANALYSIS OF ETHOXYLATED ALCOHOLS, Journal of liquid chromatography & related technologies, 19(7), 1996, pp. 1013-1032
Citations number
44
Categorie Soggetti
Chemistry Analytical","Biochemical Research Methods
Journal title
Journal of liquid chromatography & related technologies → ACNP
ISSN journal
10826076
Volume
19
Issue
7
Year of publication
1996
Pages
1013 - 1032
Database
ISI
SICI code
1082-6076(1996)19:7<1013:OCOTEL>2.0.ZU;2-M
Abstract
Influence of the temperature of a drift tube and flow rate of nitrogen as nebulizing gas with 100% hexane and 40% hexane plus 60% (5% H2O in 2-propanol) as mobile phases on the respones of ELS detector for sele cted standards of ethoxylated alcohols was examined, For optimal condi tions (1.5 dm(3) N-2/min, 50 degrees C) calibration curves for both mo bile phases were created. The response of ELSD for standards not under going evaporation is mainly affected by the composition of the mobile phase.