Mechanically alloyed Cu-Co (5-90 wt. % Co) has been analyzed using X-r
ay diffractometry to study microstructural features. All compositions
were single phase face-centered cubic. Although some of the observed p
eak broadening can be attributed to fine grain size and microstrain ef
fects, anomalous hkl-dependent peak broadening and peak shifts are cle
arly associated with stacking faults. Furthermore, the true grain size
s were > 100 nm, 3-10 times the grain size calculated without consider
ing stacking fault contributions.