SYNTHESIS OF 6-HYDROXY-2-METHYL-3-THIOXO-2H-1,2,4-TRIAZIN-5-ONE

Authors
BRANCH CL EGGLESTON DS HALTIWANGER RC KAURA AC TYLER JW
Citation
Cl. Branch et al., SYNTHESIS OF 6-HYDROXY-2-METHYL-3-THIOXO-2H-1,2,4-TRIAZIN-5-ONE, Synthetic communications, 26(11), 1996, pp. 2075-2084
Citations number
13
Categorie Soggetti
Chemistry Inorganic & Nuclear
Journal title
Synthetic communications → ACNP
ISSN journal
00397911
Volume
26
Issue
11
Year of publication
1996
Pages
2075 - 2084
Database
ISI
SICI code
0039-7911(1996)26:11<2075:SO6>2.0.ZU;2-A
Abstract
The title compound has been prepared in three steps from 2-methylthios emicarbazide following acylation, cyclisation and cation exchange chro matography. It was fully characterised by the usual spectroscopic mean s as well as by N-15 nmr spectroscopy and X-ray crystallographic analy sis.