HYDROLYSIS OF TRIFLUOROACETYLACETONE SALI CYLHYDRAZONE - STRUCTURE OFACETONE SALICYLHYDRAZONE

Authors
KRAUDELT H LUDWIG E SCHILDE U UHLEMANN E
Citation
H. Kraudelt et al., HYDROLYSIS OF TRIFLUOROACETYLACETONE SALI CYLHYDRAZONE - STRUCTURE OFACETONE SALICYLHYDRAZONE, Zeitschrift fur Naturforschung. B, A journal of chemical sciences, 51(4), 1996, pp. 563-566
Citations number
10
Categorie Soggetti
Chemistry Inorganic & Nuclear","Chemistry Inorganic & Nuclear
Journal title
Zeitschrift fur Naturforschung. B, A journal of chemical sciences → ACNP
ISSN journal
09320776
Volume
51
Issue
4
Year of publication
1996
Pages
563 - 566
Database
ISI
SICI code
0932-0776(1996)51:4<563:HOTSC->2.0.ZU;2-G
Abstract
The reaction of trifluoroacetylacelone with salicylhydrazone gives ace tone salicylhydrazone besides the expected trifluoroacetylacetone sali cylhydrazone. The resulting mixture was analyzed by mass spectroscopy. The structure of acetone salicylhydrazone was determined by X-ray ana lysis. Crystal data: a = 12,8493(12) Angstrom, b = 6,1084(8) Angstrom, c = 12,757(3) Angstrom; space group Pna2(1); Z = 4; R = 0,051; 750 un ique reflexions.