SUPPORTED CATALYST FOR SYNTHESIS OF N-PHE NYLMALEIMIDE

Citation
Y. Kita et al., SUPPORTED CATALYST FOR SYNTHESIS OF N-PHE NYLMALEIMIDE, Nippon kagaku kaishi, (3), 1996, pp. 269-274
Citations number
6
Categorie Soggetti
Chemistry
Journal title
ISSN journal
03694577
Issue
3
Year of publication
1996
Pages
269 - 274
Database
ISI
SICI code
0369-4577(1996):3<269:SCFSON>2.0.ZU;2-5
Abstract
A nem supported catalyst system Mas proposed to produce N-phenylmaleim ide (PMI) from N-phenylmaleamic acid (PMA) in an improved yield. Follo wings are important factors to affect the yield of PMI according io co nsideration of the details of dehydration process of PMA. 1) interfaci al area between the organic solvent phase and the catalyst phase. 2) T hickness of the catalyst phase. 3) Agitation. The supported catalyst i mproved considerably the yield of PMI under optimum conditons or I) an d 2). It Nas proved that a suppress of the hydrolysis of PMA in former half of the reaction brought about the high yield.