X-RAY CRYSTAL-STRUCTURE OF TRANS-DICHLOROBIS(2,6-LUTIDINE)PALLADIUM(II)

Citation
P. Losier et al., X-RAY CRYSTAL-STRUCTURE OF TRANS-DICHLOROBIS(2,6-LUTIDINE)PALLADIUM(II), Journal of chemical crystallography, 26(4), 1996, pp. 301-303
Citations number
15
Categorie Soggetti
Crystallography,Spectroscopy
ISSN journal
10741542
Volume
26
Issue
4
Year of publication
1996
Pages
301 - 303
Database
ISI
SICI code
1074-1542(1996)26:4<301:XCOT>2.0.ZU;2-R
Abstract
The X-ray structure of trans-(2,6-lutidine)(2)PdCl2 has been determine d. Golden orange crystals of the complex crystallize in the triclinic space group <P(1)over bar>, with cell dimensions a = 7.6950(8), b = 7. 9705(10), c = 8.0485(8)Angstrom, alpha = 116.967(9), beta = 113.343(8) , and gamma = 93.836(9)degrees; V = 385.18(7)Angstrom(3) and Z = 2. 13 36 unique reflections with I-net > 30 (I) on refinement afforded value s of R = 0.018 and R(w) = 0.023.