INFLUENCE OF AN OXIDIZING IMPURITY ON PREPARATION OF 2-LITHO-1,3-DITHIANE - ISOLATION OF BIS[2-(1,3-DITHIANYL)]METHANOL

Authors
ARGADE NP HAZRA BG JOSHI PL
Citation
Np. Argade et al., INFLUENCE OF AN OXIDIZING IMPURITY ON PREPARATION OF 2-LITHO-1,3-DITHIANE - ISOLATION OF BIS[2-(1,3-DITHIANYL)]METHANOL, Synthetic communications, 26(15), 1996, pp. 2797-2802
Citations number
21
Categorie Soggetti
Chemistry Inorganic & Nuclear
Journal title
Synthetic communications → ACNP
ISSN journal
00397911
Volume
26
Issue
15
Year of publication
1996
Pages
2797 - 2802
Database
ISI
SICI code
0039-7911(1996)26:15<2797:IOAOIO>2.0.ZU;2-E
Abstract
Bis-dithianylalkanols and dimers are formed in preparation of 2-lithio -1,3-dithianes due to the presence of oxidising impurity in n-BuLi (pe rhaps n-BuOOLi).