DEVELOPMENT OF HELIUM ICP-MS USING AN ENH ANCED VORTEX FLOW TORCH

Citation
A. Okino et al., DEVELOPMENT OF HELIUM ICP-MS USING AN ENH ANCED VORTEX FLOW TORCH, Bunseki Kagaku, 45(6), 1996, pp. 473-478
Citations number
14
Categorie Soggetti
Chemistry Analytical
Journal title
ISSN journal
05251931
Volume
45
Issue
6
Year of publication
1996
Pages
473 - 478
Database
ISI
SICI code
0525-1931(1996)45:6<473:DOHIUA>2.0.ZU;2-M
Abstract
To overcome some problems of the argon ICP-MS, a helium ICP-MS device was developed using an enhanced vortex flow torch. Effects of sampler- skimmer distance on the pressure in the 2nd stage and on the ion signa l intensities were studied and it was found that both the Mach disk po sition and the most suitable position for analysis are 7 mm. No backgr ound spectral peak was found at m/z values over 32 except for copper f rom the sampler. Ion intensities of neon and krypton that were low in sensitivity in argon ICP-MS due to their high ionization energies were as much as 36 and 24 times greater in He ICP-MS, respectively.