R. Gunther et al., DETERMINATION OF CONCENTRATION DEPTH PROFILES USING TOTAL-REFLECTION X-RAY-FLUORESCENCE SPECTROMETRY IN COMBINATION WITH ION-BEAM ETCHING, Review of scientific instruments, 67(6), 1996, pp. 2332-2336
A new method for quantitative concentration depth profiling is present
ed. It combines a sputter-etching technique with ex situ total-reflect
ion x-ray fluorescence analysis. It allows quantitative depth-resolved
analysis of alloys consisting of elements with atomic number greater
than or equal to 13. Basic requirements for a high depth resolution ar
e reported. With this method, an experimental depth resolution of 1.4
(+/- 0.4) nm is obtained that is comparable with the best achievable r
esults from other depth profiling methods. (C) 1996 American Institute
of Physics.