CHARACTERIZATION OF SAPO-11 SYNTHESIZED CONVENTIONALLY AND IN THE PRESENCE OF FLUORIDE IONS

Authors
SINGH PS BANDYOPADHYAY R RAO BS
Citation
Ps. Singh et al., CHARACTERIZATION OF SAPO-11 SYNTHESIZED CONVENTIONALLY AND IN THE PRESENCE OF FLUORIDE IONS, Journal of the Chemical Society. Faraday transactions, 92(11), 1996, pp. 2017-2026
Citations number
36
Categorie Soggetti
Chemistry Physical","Physics, Atomic, Molecular & Chemical
Journal title
Journal of the Chemical Society. Faraday transactions → ACNP
ISSN journal
09565000
Volume
92
Issue
11
Year of publication
1996
Pages
2017 - 2026
Database
ISI
SICI code
0956-5000(1996)92:11<2017:COSSCA>2.0.ZU;2-Q
Abstract
SAPO-11 samples have been synthesized by the conventional route and fr om an aqueous solution containing F- anions. Characterization of these samples by X-ray diffraction (XRD), chemical analysis, X-ray photoele ctron spectroscopy (XPS), thermal analysis, NMR, adsorption measuremen ts and catalytic test reaction reveals that the samples are highly cry stalline, but differ in some physico-chemical properties. These differ ences in the properties of SAPO-11 obtained via different synthesis ro utes are correlated with different ordering of silicon substitution wi thin the framework.