A. Fonseca et al., OPTIMIZATION OF CATALYTIC PRODUCTION AND PURIFICATION OF BUCKYTUBES, Journal of molecular catalysis. A, Chemical, 107(1-3), 1996, pp. 159-168
Carbon nanotubes were produced in large amounts by catalytic decomposi
tion of acetylene in the presence of supported Co and Fe catalysts. Th
e influence of various parameters such as the way of catalyst preparat
ion, the nature of the support, the size of active metal particles, an
d the reaction conditions on the buckytube formation was studied. The
process was optimized towards the large-scale production of buckytubes
having the same diameters as the fullerene nanotubes obtained from th
e are-discharge method. The separation of the buckytubes from the cata
lyst was also achieved.