Z. Li et al., MICROSCOPIC ANALYSIS OF DEFECTS IN A HIGH-RESISTIVITY SILICON DETECTOR IRRADIATED TO 1.7X10(15)N CM(2)/, IEEE transactions on nuclear science, 43(3), 1996, pp. 1590-1598
Current-based microscopic defect analysis methods with optical filling
techniques, namely current deep level transient spectroscopy (I-DLTS)
and thermally stimulated current (TSC), have been used to study defec
t levels in a high resistivity silicon detector (p(+)-n-n(+)) induced
by very high fluence neutron (VHFN) irradiation (1.7x10(15) n/cm(2)).
As many as fourteen deep levels have been detected by I-DLTS. Arrheniu
s plots of the I-DLTS data have shown defects with energy levels rangi
ng from 0.03 eV to 0.5 eV in the energy band gap. Defect concentration
s of relatively shallow levels (E(t) < 0.33 eV) are in the order of 10
(13)cm(-3), while those for relatively deep levels (E(t) > 0.33 eV) ar
e in the order of 10(14) cm(-3). TSC data have shown similar defect sp
ectra. A full depletion voltage of about 27,000 volts has been estimat
ed by C-V measurements for the as-irradiated detector, which correspon
ds to an effective space charge density (N-eff) in the order of 2x10(1
4) cm(-3). Both detector leakage current and full depletion voltage ha
ve been observed to increase with elevated temperature annealing (ETA)
. The increase of the full depletion voltage corresponds to the increa
se of some deep levels, especially the 0.39 eV level. Results of posit
ron annihilation spectroscopy have shown a decrease of total concentra
tion of vacancy related defects including vacancy clusters with ETA, s
uggesting the breaking up of vacancy clusters as possible source of va
cancies for the formation of single defects during the reverse anneal.