Y. Vonkaenel et al., A NEW INTERPRETATION OF BULGE TEST MEASUREMENTS USING NUMERICAL-SIMULATION, DIAMOND AND RELATED MATERIALS, 5(6-8), 1996, pp. 635-639
Analysis of the deflection of a circular membrane under differential p
ressure (bulge test) is a well-known method of determining the elastic
properties of thin films. However, analytical models always suffer fr
om simplifying hypotheses. In this study we present a new approach, ba
sed on numerical modeling, to interpret pressure-deflection curves. By
adjusting Young's modulus and Poisson's ratio in the simulation progr
am, it is possible to reproduce the experimental curves faithfully. Th
e method was successfully tested with two different materials (silicon
and aluminium) with known elastic properties and was then used to det
ermine biaxial Young's moduli of CVD diamond thin films for three diff
erent microstructures. The values of E varied from 565 to 620 GPa (ass
umin,g a Poisson ratio of 0.1). Grain boundaries are thought to be res
ponsible for the relatively low values of Young's moduli. Uncertaintie
s in E are relatively large (10%-15%) because the method is highly sen
sitive to experimental parameters such as thickness or membrane diamet
er and to the initial residual stress state which is known only approx
imately.