E. Jansen et al., THERMAL-CONDUCTIVITY MEASUREMENTS ON DIAMOND FILMS BASED ON MICROMECHANICAL DEVICES, DIAMOND AND RELATED MATERIALS, 5(6-8), 1996, pp. 644-648
An accurate technique to measure the thermal conductivity k(T) of CVD
diamond based on new micromechanical devices is presented. The thermal
conductivity parallel to the surface of films with thicknesses rangin
g from 2 to several hundred mu m can be determined over a wide tempera
ture range. The diamond films were patterned by RIE in an oxygen plasm
a to achieve accurate device dimensions. The silicon was completely re
moved from a defined area leaving diamond membranes and free standing
diamond cantilevers. A thin film heater generated a temperature profil
e which was measured using several thermoresistors. Shape and dimensio
ns of the structures were optimized using computer simulations (FEA).
The effects of thermal radiation, additional metallization and insulat
ion layers were minimized. Measurements on CZ silicon show a very good
agreement with literature results. The thermal conductivity of diamon
d films with thicknesses between 3.6 and 8 mu m grown on a silicon sub
strate by the hot filament technique with different methane concentrat
ions were measured between -195 and 300 degrees C. The measured values
range between < 1 and 5 W cm(-1) K-1.