Jp. Douzals et al., MICROSCOPIC STUDY OF STARCH GELATINIZATION UNDER HIGH HYDROSTATIC-PRESSURE, Journal of agricultural and food chemistry, 44(6), 1996, pp. 1403-1408
Starch gelatinization corresponds to a melting phase transition in aqu
eous medium. Such a transition involves important mass transfer of wat
er. Using a high-pressure bomb including optical ports, the volume var
iation of starch granules in suspension was related to gelatinization
during a high-pressure treatment up to 420 MPa. Microscopic observatio
ns of wheat and potato starch granules were compared with macroscopic
measurements of compressibility up to 600 MPa and gelatinization inten
sity using differential scanning calorimetry on treated suspensions. W
heat starch gelatinization started below 300 MPa and was completely ac
hieved at 600 MPa. Potato starch was not altered under 600 MPa. The be
havior of the volume variation of starch granules under pressure compa
red with starch suspensions compressibility could be explained by simu
ltaneous compression and hydration mechanisms.