Rw. Armstrong et al., ELASTIC, PLASTIC AND CRACKING INDENTATION BEHAVIOR OF SILICON-CRYSTALS, Materials science & engineering. A, Structural materials: properties, microstructure and processing, 209(1-2), 1996, pp. 91-96
The ambient temperature indentation hardness properties of silicon cry
stals have been studied over the full range of their nanoscale elastic
/plastic and microscale elastic/plastic/cracking behaviors. The materi
al properties are interpreted on the basis of applied force versus res
idual indentation size or crack size measurements and, also, on the ba
sis of computed hardness stress-strain dependencies. Cracking, when it
occurs, is attributed to sessile dislocation reactions that are initi
ated at microslip system intersections. Significant hardening was reve
aled in nanoindentation tests of carbon-ion implanted material, partic
ularly, for crack-free plastic deformation obtained when silicon carbi
de was formed in the crystal surface layer by high temperature implant
ation. Otherwise, continuous force vs. displacement curves were employ
ed to track the occurrence of cracking during indenter loading and cra
ck growth on unloading, as facilitated in the latter case by the resid
ual plastic deformation produced during the loading part of the hardne
ss cycle.