Jm. Lopezvillegas et al., STRUCTURE AND NONUNIFORM STRAIN ANALYSIS ON P-TYPE POROUS SILICON BY X-RAY REFLECTOMETRY AND X-RAY-DIFFRACTION, Thin solid films, 276(1-2), 1996, pp. 238-240
Structural properties of porous silicon layers performed on p-type (10
0) silicon wafers have been studied by X-ray reflectometry and X-ray d
iffraction techniques. The mean surface porosity of the layers has bee
n obtained by comparing the critical reflection angles of the porous l
ayer and the silicon substrate. The obtained values are in agreement w
ith microgravimetry measurements. The strain of the porous layer as a
function of the technological parameters has been analyzed by X-ray di
ffraction. The origin of the strain in the porous silicon is discussed
according to the presence of stress and changes in the porosity acros
s the layer. Finally, a minimum strain condition has been found, allow
ing the optimization of the fabrication process.