C. Masciovecchio et al., A PERFECT CRYSTAL X-RAY ANALYZER WITH MEV ENERGY RESOLUTION, Nuclear instruments & methods in physics research. Section B, Beam interactions with materials and atoms, 111(1-2), 1996, pp. 181-186
We present a new method to construct a spherical crystal X-ray energy
analyser. The energy analysis is based on high order Bragg reflections
from a silicon perfect crystal at angles very close to 90 degrees. In
order to preserve the perfect crystal properties in a focusing optics
, necessary for meV energy resolution and large angular acceptance, we
developed a procedure to mount approximate to 12000 small crystals, o
btained from the same silicon wafer, on a spherical substrate. The met
hod is based on computer controlled glueing and cycles of etching for
each crystal. We obtained analysers with an energy resolution of 1.7+/
-0.5 meV for 21.75 keV X-rays, using the Si(11 11 11) reflection, and
with 25 mrad(2) angular acceptance. These analysers have been specific
ally developed for high energy resolution inelastic X-ray scattering.