A PERFECT CRYSTAL X-RAY ANALYZER WITH MEV ENERGY RESOLUTION

Citation
C. Masciovecchio et al., A PERFECT CRYSTAL X-RAY ANALYZER WITH MEV ENERGY RESOLUTION, Nuclear instruments & methods in physics research. Section B, Beam interactions with materials and atoms, 111(1-2), 1996, pp. 181-186
Citations number
15
Categorie Soggetti
Physics, Nuclear","Nuclear Sciences & Tecnology","Instument & Instrumentation
ISSN journal
0168583X
Volume
111
Issue
1-2
Year of publication
1996
Pages
181 - 186
Database
ISI
SICI code
0168-583X(1996)111:1-2<181:APCXAW>2.0.ZU;2-C
Abstract
We present a new method to construct a spherical crystal X-ray energy analyser. The energy analysis is based on high order Bragg reflections from a silicon perfect crystal at angles very close to 90 degrees. In order to preserve the perfect crystal properties in a focusing optics , necessary for meV energy resolution and large angular acceptance, we developed a procedure to mount approximate to 12000 small crystals, o btained from the same silicon wafer, on a spherical substrate. The met hod is based on computer controlled glueing and cycles of etching for each crystal. We obtained analysers with an energy resolution of 1.7+/ -0.5 meV for 21.75 keV X-rays, using the Si(11 11 11) reflection, and with 25 mrad(2) angular acceptance. These analysers have been specific ally developed for high energy resolution inelastic X-ray scattering.