An ATR reflectometer was constructed using a twin goniometer system an
d lock-in detection technique. The angular resolution was +/-0.015 deg
rees, determined by the beam divergence of the He-Ne and YAG laser lig
ht sources, while the error in reflectivity was less than +/-2%. The a
ngular distribution of the ATR reflection and backward resonance light
emission was measured in evaporated silver and gold films of 30-90 nm
thickness with both wavelengths (0.6382 and 1.064 mu m). Exact roughn
ess spectrums were determined by a fitting procedure using the Kroger-
Kretschmann formulae. A relatively sharp thickness dependence was foun
d in the components of the dielectric constant at both wavelengths.