Ap. Jephcoat et Sp. Besedin, TEMPERATURE-MEASUREMENT AND MELTING DETERMINATION IN THE LASER-HEATEDDIAMOND-ANVIL CELL, Philosophical transactions-Royal Society of London. Physical sciences and engineering, 354(1711), 1996, pp. 1333-1360
We discuss the problems associated with the measurement of temperature
and the determination of melting in the laser-heated diamond-anvil ce
ll. We also briefly summarize the main developments of the last three
decades in simultaneous high-P-T measurements and review practical asp
ects of the technique. The melting curve of argon as a function of pre
ssure has been determined up to 47 GPa, and within experimental error,
agrees with a Simon relation extrapolation of the melting curve from
previous data to only 1.1 GPa. On the basis of currently debated upper
and lower limits for the melting curve of pure iron, the argon meltin
g curve can intersect the melting curve of iron in the range 40-65 GPa
. Our experiments suggest that the melting points of iron and argon ar
e equal at 47 +/- 1.0 GPa and 2750 +/- 200 K. Above this pressure, pur
e iron would be expected to melt at a lower temperature than solid arg
on. In a separate experiment, the melting temperature of iron in an ar
gon medium at 57 +/- 1 GPa appears greater than 2650 +/- 200 K. The in
tersection of the melting curves for non-interacting materials could s
erve as standard P-T fixed-points and offer a route to the standardiza
tion of different methods of temperature measurement.