H. Kutami et al., STRUCTURE REFINEMENT OF A TWIN-FREE ORTHORHOMBIC YBA2CU3OX SINGLE-CRYSTAL PREPARED BY SRL-CP METHOD, Physica. C, Superconductivity, 262(3-4), 1996, pp. 173-176
A pure single crystal has been grown by the Solute Rich Liquid-Crystal
Pulling Method (SRL-CP method), and a superconductive twin-free YBa2C
u3Ox single crystal has been obtained by means of annealing the twinne
d crystal at 400 degrees C with a uni-axial compression in an oxygen a
tmosphere. SQUID magnetization-temperature measurement on the twin-fre
e crystal shows the onset T-c at 88 K. Single-crystal X-ray technique
was used to conduct structure refinement of the crystal at 296 K (room
temperature).