Friction force microscopy (FFM) was used to study microscale friction
between a sharp tip and various samples. Effect of normal load and tip
material on the coefficient of friction has been studied. Friction fo
rce as a function of normal load of vir in silicon with a thin film of
native oxide and dry-oxidized SiO2 coating showed two distinct slopes
. The coefficient of friction in the low load region of less than abou
t 15 mN is lower than that in the high load region. The critical load
at which the coefficient of friction starts to increase corresponds to
the specimen hardness. Ploughing at high loads is believed to be resp
onsible for high values of the coefficient of friction. The coefficien
t of friction of polished natural diamond remains virtually independen
t of normal load because no ploughing occurs. The coefficient of frict
ion on a macroscale is higher than that on a microscale for comparable
contact stresses. When measured for the small apparent area of contac
t and very small loads used in microscale measurements, the indentatio
n hardness and modulus of elasticity on a microscale are higher than t
hat at the macroscale. This reduces the degree of wear at the microsca
le. In addition, small apparent areas of contact in microscale measure
ments reduces the number of particles trapped at the interface and thu
s minimizes the ploughing contribution to the friction force. Based on
this study, it is concluded that measured values of the coefficient o
f friction on a microscale are a strong function of normal load and th
e apparent area of contact. Ultralow values of the coefficient of fric
tion and near-zero wear can be achieved with microscale components at
very light loads in the absence of significant ploughing.