DETERMINATION OF LOWER THIOLS IN ATMOSPHERIC AIR

Citation
Ys. Drugov et al., DETERMINATION OF LOWER THIOLS IN ATMOSPHERIC AIR, Journal of analytical chemistry, 51(6), 1996, pp. 595-601
Citations number
23
Categorie Soggetti
Chemistry Analytical
ISSN journal
10619348
Volume
51
Issue
6
Year of publication
1996
Pages
595 - 601
Database
ISI
SICI code
1061-9348(1996)51:6<595:DOLTIA>2.0.ZU;2-K
Abstract
A procedure for determining lower thiols in atmospheric air at a level of maximum permissible concentrations is proposed. The procedure is b ased on the extraction of thiol impurities from air in a trap with a p olymer sorbent at room temperature, the thermal desorption of the conc entrated impurities, and their determination on a chromatograph with a flame-photometric or photoionization detector. The procedure makes it possible to determine 0.2-6 ng of thiols C-1-C-4 with a relative stan dard deviation of 25-34%.