T. Shiogai et al., THE EFFECT OF MICROSTRUCTURES OF SIALON C ERAMICS ON FATIGUE PROPERTIES AT ROOM-TEMPERATURE, Nippon Seramikkusu Kyokai gakujutsu ronbunshi, 104(6), 1996, pp. 562-566
The effect of microstructure on the fatigue behavior at room temperatu
re in air was studied using sialon ceramics with different microstruct
ures prepared by selecting starting raw materials and sintering condit
ions. Dynamic, static and cyclic fatigue tests were carried out on smo
oth specimens by the 3-point bending method, Oxide content in the inte
rgranular phase and grain size affectted the dynamic fatigue behavior.
Remarkable slow crack growth attributable to the stress corrosion by
humidity in air was observed in the sample with elongated grains, In s
tatic fatigue tests, the observed lifetime of each sample was in agree
ment with that predicted from dynamic fatigue properties, and the crac
k propagated through the intergranular phase. The acceleration of fati
gue was observed under cyclic loading. The accelerative effects on cyc
lic fatigue was significant in the sample with coarse grains, Sialon c
eramics with elongated grains prepared by HIP showed both high fractur
e toughness and high strength, but the fatigue parameter ''n'' was low
and the acceleration of fatigue under cyclic loading was significant
because of its coarse grains.