MAGIC-ANGLE-SPINNING NMR - A VALUABLE TOOL FOR MONITORING THE PROGRESS OF REACTIONS IN SOLID-PHASE SYNTHESIS

Authors
WEHLER T WESTMAN J
Citation
T. Wehler et J. Westman, MAGIC-ANGLE-SPINNING NMR - A VALUABLE TOOL FOR MONITORING THE PROGRESS OF REACTIONS IN SOLID-PHASE SYNTHESIS, Tetrahedron letters, 37(27), 1996, pp. 4771-4774
Citations number
15
Categorie Soggetti
Chemistry Inorganic & Nuclear
Journal title
Tetrahedron letters → ACNP
ISSN journal
00404039
Volume
37
Issue
27
Year of publication
1996
Pages
4771 - 4774
Database
ISI
SICI code
0040-4039(1996)37:27<4771:MN-AVT>2.0.ZU;2-Q
Abstract
Proton NMR-spectra of four different solid supports were obtained usin g the magic angle spinning Nano NMR probe to evaluate their utility in solid phase chemistry. It was possible to analyse the spectra in resp ect to structure and quantity. An intramolecular cyclisation reaction on the solid support in the Nano tube could be followed directly. Copy right (C) 1996 Elsevier Science Ltd