SYNTHESIS AND X-RAY-ANALYSIS OF 1-((1S)-PHENYLETHYL)-AZETIDINE-(2R)-PIPERIDINAMIDE

Authors
DEGELDER R SMITS JMM STARMANS WAJ THIJS L ZWANENBURG B
Citation
R. Degelder et al., SYNTHESIS AND X-RAY-ANALYSIS OF 1-((1S)-PHENYLETHYL)-AZETIDINE-(2R)-PIPERIDINAMIDE, Journal of chemical crystallography, 26(9), 1996, pp. 639-642
Citations number
13
Categorie Soggetti
Crystallography,Spectroscopy
Journal title
Journal of chemical crystallography → ACNP
ISSN journal
10741542
Volume
26
Issue
9
Year of publication
1996
Pages
639 - 642
Database
ISI
SICI code
1074-1542(1996)26:9<639:SAXO1>2.0.ZU;2-H
Abstract
The crystal and molecular structure of a new azetidine-2-carboxylic am ide derivative is described. The structure was solved by direct method s and refined by least squares methods to R1 = 0.0393 for 4264 reflect ions (with I > 2 sigma(I)). The structure consists of two independent molecules which are chemically the same with slight differences in geo metry. Crystal data: C17H24N2O, monoclinic, space group P2(1), a = 8.3 782(4), b = 20.0342(13), c = 9.7769(8)Angstrom, beta = 109.687(6)degre es, V = 1545.1(2)Angstrom(3), Z = 4.