S. Pascarelli et al., X-RAY OPTICS OF A DYNAMICAL SAGITTAL-FOCUSING MONOCHROMATOR ON THE GILDA BEAMLINE AT THE ESRF, Journal of synchrotron radiation, 3, 1996, pp. 147-155
The performance of a dynamical sagittal-focusing monochromator for har
d X-rays is described. It consists of a flat first crystal and a diamo
nd-shaped ribbed second crystal which is clamped by its central rib an
d dynamically bent by applying a force on its two apices. The system h
as proved to perform very well on the GILDA beamline at the ESRF. The
horizontal acceptance varies with energy and with focusing geometry as
predicted theoretically; :he total available horizontal fan of radiat
ion (3.6 mrad) is in fact collected in the 1:3 geometry. The system is
routinely run in a dynamical focusing mode for XAFS spectroscopy in t
he energy range 5-30 keV with Si(311) crystals, with a constant spot s
ize FWHM similar to 1 mm on the sample and without degradation of ener
gy resolution or reproducibility. Using simple geometrical considerati
ons we calculate the variations of the horizontal profile of the refle
cted beam during rocking-curve scans in different focusing geometries
and find them in agreement with observed ones. Not only is this is a p
ractical aid in alignment but it illustrates the X-ray optics of sagit
tal focusing in an elegant way.