SYNTHESIS AND CHARACTERIZATION OF A NOVEL MICROPOROUS ALUMINOPHOSPHATE ALPO4-JDF (2ALPO4-CENTER-DOT-HOCH2CH2NH2) FROM ALCOHOL SYSTEMS

Citation
Qm. Gao et al., SYNTHESIS AND CHARACTERIZATION OF A NOVEL MICROPOROUS ALUMINOPHOSPHATE ALPO4-JDF (2ALPO4-CENTER-DOT-HOCH2CH2NH2) FROM ALCOHOL SYSTEMS, Journal of materials chemistry, 6(7), 1996, pp. 1207-1210
Citations number
22
Categorie Soggetti
Chemistry Physical","Material Science
ISSN journal
09599428
Volume
6
Issue
7
Year of publication
1996
Pages
1207 - 1210
Database
ISI
SICI code
0959-9428(1996)6:7<1207:SACOAN>2.0.ZU;2-0
Abstract
The synthesis of a novel aluminophosphate microporous compound AIPO(4) -JDF (where J means Jilin University and DF is Davy Faraday Laboratory ) containing organic amine in the presence of the template HOCH2CH2NH2 from predominantly non-aqueous media is described. Chemical and eleme ntal analyses disclosed its idealized formula as 2AlPO(4) . HOCH2CH2NH 2. AIPO(4)-JDF has been characterized by X-ray powder diffraction (XRD ), IR spectroscopy, scanning electron microscopy (SEM), differential t hermal analysis (DTA) and thermogravimetry (TG), and magic angle spinn ing nuclear magnetic resonance (MAS NMR) spectroscopy.