Qm. Gao et al., SYNTHESIS AND CHARACTERIZATION OF A NOVEL MICROPOROUS ALUMINOPHOSPHATE ALPO4-JDF (2ALPO4-CENTER-DOT-HOCH2CH2NH2) FROM ALCOHOL SYSTEMS, Journal of materials chemistry, 6(7), 1996, pp. 1207-1210
The synthesis of a novel aluminophosphate microporous compound AIPO(4)
-JDF (where J means Jilin University and DF is Davy Faraday Laboratory
) containing organic amine in the presence of the template HOCH2CH2NH2
from predominantly non-aqueous media is described. Chemical and eleme
ntal analyses disclosed its idealized formula as 2AlPO(4) . HOCH2CH2NH
2. AIPO(4)-JDF has been characterized by X-ray powder diffraction (XRD
), IR spectroscopy, scanning electron microscopy (SEM), differential t
hermal analysis (DTA) and thermogravimetry (TG), and magic angle spinn
ing nuclear magnetic resonance (MAS NMR) spectroscopy.