Jn. Chen et al., A STUDY ON THE PREPARATION, STRUCTURE, AND PROPERTIES OF MICROCRYSTALLINE CELLULOSE, Journal of macromolecular science. Pure and applied chemistry, A33(12), 1996, pp. 1851-1862
The preparation, structure, and properties of microcrystalline cellulo
se (MCC) from rice straw were investigated by IR, x-ray, viscometry, p
olarizing microscope, SEM, etc. The results are as follows: 1. The lev
eling-off degree of polymerization (LODP) obtained from rice straw is
about 80-150. The dimensions of MCC granules are 20-30 mu m length, 0.
5-0.8 mu m thick, and the crystallinity is about 80%. 2. The aqueous s
uspension of a certain concentration of MCC can form a gel under the e
ffect of shear force. The viscosity of MCC gel increased with an incre
asing content of MCC in water. A sharper increase of viscosity occurre
d in the 3-6% range. 3. The addition of one or two valence salts into
the MCC gel increased the viscosity. 4. The viscosity of MCC gel has i
ts maximum value at pH 8. 5. The MCC gel as an emulsifying agent can f
orm a stable emulsion in the oil/water system when the ratio of oil/wa
ter is below 6/4.