M. Itsumi et al., COPPER DECORATION FOLLOWED BY TEM OBSERVATION DEFECTS IN THE BURIED OXIDES OF SOI SUBSTRATES, Journal of the Electrochemical Society, 143(7), 1996, pp. 2357-2361
Copper decoration followed by transmission electron microscopy (TEM) o
bservation is proposed for identifying defects in the buried oxides of
silicon-on-insulator (SOI) substrates. This method comprises Si surfa
ce layer etching (i.e., exposure of the buried-oxide surface), oxide-d
efect location detection with copper decoration, and sample thinning f
or TEM observation and analysis. The advantage of copper decoration is
that the electronic current needed for defect detection is very small
, so the influence of the electronic current on the original oxide-def
ect structure can be minimized. Defects observed are categorized into
four groups from the viewpoint of size and shape.